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1.
LA‐ICP‐MS is increasingly applied to obtain quantitative multi‐element data with minimal sample preparation, usually achieved by calibration using reference materials (RMs). However, some ubiquitous RMs, for example the NIST SRM 61× series glasses, suffer from reported value uncertainties for certain elements. Moreover, no long‐term data set of analyses conducted over a range of ablation and tuning conditions exists. Thus, there has been little rigorous examination of the extent to which offsets between measured and reported values are the result of error in these values rather than analytically induced fractionation. We present new software (‘LA‐MINE’), capable of extracting LA‐ICP‐MS data with no user input, and apply this to our system, yielding over 5 years of data (~ 5700 analyses of ten glass and carbonate RMs). We examine the relative importance of systematic analytical bias and possible error in reported values through a mass‐specific breakdown of fourteen of the most commonly determined elements. Furthermore, these data, obtained under a wide range of different ablation conditions, enable specific recommendations of how data quality may be improved, for example the role of diatomic gas, the effect of differential inter‐glass fractionation factors and choice of transport tubing material. Finally, these data demonstrate that the two‐volume Laurin ablation cell is characterised by no discernible spatial heterogeneity in measured trace element ratios.  相似文献   
2.
The goal of this contribution is to focus on improving the quality of gravity field models in the form of spherical harmonic representation via alternative configuration scenarios applied in future gravimetric satellite missions. We performed full-scale simulations of various mission scenarios within the frame work of the German joint research project “Concepts for future gravity field satellite missions” as part of the Geotechnologies Program, funded by the German Federal Ministry of Education and Research and the German Research Foundation. In contrast to most previous simulation studies including our own previous work, we extended the simulated time span from one to three consecutive months to improve the robustness of the assessed performance. New is that we performed simulations for seven dedicated satellite configurations in addition to the GRACE scenario, serving as a reference baseline. These scenarios include a “GRACE Follow-on” mission (with some modifications to the currently implemented GRACE-FO mission), and an in-line “Bender” mission, in addition to five mission scenarios that include additional cross-track and radial information. Our results clearly confirm the benefit of radial and cross-track measurement information compared to the GRACE along-track observable: the gravity fields recovered from the related alternative mission scenarios are superior in terms of error level and error isotropy. In fact, one of our main findings is that although the noise levels achievable with the particular configurations do vary between the simulated months, their order of performance remains the same. Our findings show also that the advanced pendulums provide the best performance of the investigated single formations, however an accuracy reduced by about 2–4 times in the important long-wavelength part of the spectrum (for spherical harmonic degrees ${<}50$ ), compared to the Bender mission, can be observed. Concerning state-of-the-art mission constraints, in particular the severe restriction of heterodyne lasers on maximum range-rates, only the moderate Pendulum and the Bender-mission are beneficial options, of course in addition to GRACE and GRACE-FO. Furthermore, a Bender-type constellation would result in the most accurate gravity field solution by a factor of about 12 at long wavelengths (up to degree/order 40) and by a factor of about 200 at short wavelengths (up to degree/order 120) compared to the present GRACE solution. Finally, we suggest the Pendulum and the Bender missions as candidate mission configurations depending on the available budget and technological progress.  相似文献   
3.
Analysis of the NWA 2086 CV3 chondrite showed a matrix/chondrule ratio of 52%, similar to Bali, Mokoia, and Grosanaja. Nearly twice as many chondrule fragments as intact ones demonstrate that an early fragmentation phase occurred prior to final accretion. After this event, no substantial mechanical change or redeposition is evident. Rims with double‐layered structures were identified around some chondrules, which, in at least one case, is attributed to an accretionary origin. The rim's outer parts with a diffuse appearance were formed by in situ chemical alteration. During this later process, Mg content decreased, Fe content increased, and olivine composition was homogenized, producing a rim composition close to that of the matrix. This alteration occasionally happened along fractures and at confined locations, and was probably produced by fluid interactions. Iron oxides are the best candidate for a small grain‐sized alteration product; however, technical limitations in the available equipment did not allow exact phase identification. These results suggest that NWA 2086 came from a location (possible more deeply buried) in the CV parent body than Mokoia or Bali, and suffered less impact effects—although there is no evidence of sustained thermal alteration. This meteorite may represent a sample of the CV parent asteroid interior and provide a useful basis for comparison with other CV meteorites in the future.  相似文献   
4.
The boloSource() algorithm is a tool to separate the signal of compact sources from that of the diffuse background in the timeline of far-infrared measurements performed by the PACS camera of the Herschel Space Observatory. An important characteristic and quality indicator of this method is that how well it can reproduce the flux of faint standard stars which have reliable flux estimates. For this propose we selected a few calibrator targets and constructed light curves by extracting point source flux for each repetition of the measurements independently using standard aperture photometry methods. These were compared with the light curves obtained using the boloSource() method on the same dataset. The results indicate that boloSource() provides a similar level of photometric accuracy and reproducibility as the usual flux extraction and photometry methods. This new technique will be developed further and also tested against other methods in more complex fields with the goal to make it usable for large-scale studies in the future.  相似文献   
5.
Magnetic resonance sounding (MRS) has increasingly become an important method in hydrogeophysics because it allows for estimations of essential hydraulic properties such as porosity and hydraulic conductivity. A resistivity model is required for magnetic resonance sounding modelling and inversion. Therefore, joint interpretation or inversion is favourable to reduce the ambiguities that arise in separate magnetic resonance sounding and vertical electrical sounding (VES) inversions. A new method is suggested for the joint inversion of magnetic resonance sounding and vertical electrical sounding data. A one‐dimensional blocky model with varying layer thicknesses is used for the subsurface discretization. Instead of conventional derivative‐based inversion schemes that are strongly dependent on initial models, a global multi‐objective optimization scheme (a genetic algorithm [GA] in this case) is preferred to examine a set of possible solutions in a predefined search space. Multi‐objective joint optimization avoids the domination of one objective over the other without applying a weighting scheme. The outcome is a group of non‐dominated optimal solutions referred to as the Pareto‐optimal set. Tests conducted using synthetic data show that the multi‐objective joint optimization approximates the joint model parameters within the experimental error level and illustrates the range of trade‐off solutions, which is useful for understanding the consistency and conflicts between two models and objectives. Overall, the Levenberg‐Marquardt inversion of field data measured during a survey on a North Sea island presents similar solutions. However, the multi‐objective genetic algorithm method presents an efficient method for exploring the search space by producing a set of non‐dominated solutions. Borehole data were used to provide a verification of the inversion outcomes and indicate that the suggested genetic algorithm method is complementary for derivative‐based inversions.  相似文献   
6.
The “TNOs are Cool!: A survey of the trans-Neptunian region” is a Herschel Open Time Key Program that aims to characterize planetary bodies at the outskirts of the Solar System using PACS and SPIRE data, mostly taken as scan-maps. In this paper we summarize our PACS data reduction scheme that uses a modified version of the standard pipeline for basic data reduction, optimized for faint, moving targets. Due to the low flux density of our targets the observations are confusion noise limited or at least often affected by bright nearby background sources at 100 and 160 \(\mu \) m. To overcome these problems we developed techniques to characterize and eliminate the background at the positions of our targets and a background matching technique to compensate for pointing errors. We derive a variety of maps as science data products that are used depending on the source flux and background levels and the scientific purpose. Our techniques are also applicable to a wealth of other Herschel solar system photometric observations, e.g. comets and near-Earth asteroids. The principles of our observing strategies and reduction techniques for moving targets will also be applicable for similar surveys of future infrared space projects.  相似文献   
7.
Cities represent thermal load areas compared with their surrounding environments. Due to climate change, summer heat events will increase. Therefore, mitigation and adaptation are needed. In this study, meteorological measurements in various local climate zones were performed to demonstrate the influence of evaporation surfaces and other factors on thermal comfort, as determined by the physiologically equivalent temperature (PET). Furthermore, a quantification of the thermal effects of several adaptation measures and varying meteorological parameters was made using model simulations (ENVI-met) in an inner-city neighborhood (Oberhausen, Germany). The results show that the most effective adaptation measure was increased wind speed (maximal 15 K PET reduction). Moreover, vegetation areas show greater PET reductions by the combination of shading and evapotranspiration than water surfaces. The creation of park areas with sufficient water supply and tall, isolated, shade-providing trees that allow for adequate ventilation can be recommended for planning.  相似文献   
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